{"id":117,"date":"2010-02-18T22:42:49","date_gmt":"2010-02-19T04:42:49","guid":{"rendered":"http:\/\/beta.solidshandlingtech.com\/?p=117"},"modified":"2017-11-10T14:02:17","modified_gmt":"2017-11-10T14:02:17","slug":"requirements-for-biomass-sampling","status":"publish","type":"post","link":"https:\/\/solidshandlingtech.com\/?p=117","title":{"rendered":"Requirements for Biomass Sampling"},"content":{"rendered":"<h2><span style=\"font-size: 12pt;\"><strong><span style=\"font-family: Arial;\"><span style=\"font-size: 14pt;\">Requirements for Biomass Sampling<\/span><br \/>\n<\/span><\/strong><span style=\"font-family: Arial;\">Guest article by Paul Janze, Sandwell Engineering<\/span><\/span><\/h2>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><strong>Introduction<\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><img loading=\"lazy\" decoding=\"async\" class=\"alignleft\" src=\"\/wp-content\/uploads\/2010\/02\/janze_sampling1.jpg\" alt=\"\" width=\"240\" height=\"210\" align=\"left\" border=\"1\" \/>With the current emphasis on the use of biomass for `green\u2019 energy purposes, the importance of having good quality `hog fuel\u2019, cannot be over-emphasized. And to ensure good quality fuel, good sampling procedures must be followed.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Woody biomass in chip form has been utilized by the pulp and paper industry for many decades and chip quality has long been recognized as having an important effect on pulp quality; to make good pulp you need good chips. Likewise for a biomass-fired plant to operate efficiently, it needs a reliable, constant supply of consistent quality fuel.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Good quality control relies on proper sampling, which must be accurate and precise and truly represent the main body of biomass. Without good sampling, quality control is based on false information. Bulk materials are difficult to sample properly on a production basis. Manual sampling can be done but it is labor intensive, prone to errors and does not easily fit into a production environment.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Collecting samples of biomass is one task not always done well, and unless the sample is taken properly, it will not be a true representation of the main product flow.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Biomass is not easy to sample. It appears in a myriad of species, forms and sizes; it knits together, doesn\u2019t flow well, consolidates and packs easily; it can have a wide range of moisture contents, basic and bulk densities and calorific values; it will freeze; it is very dusty, catches fire easily and is self-combustible; it can contain all manner of contaminants; it can be quite fragile and care must be taken not to degrade the material.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">To be of value, biomass samples need to be unbiased, accurate, precise and representative of the main lot or consignment of material.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">The intent of this paper is to summarize the requirements that must be met in order to provide representative chip sampling and to do so in an easily understood and achievable manner. This paper does not consider chip classification or analysis.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><strong>1.\u00a0 Features of Good Sampling<\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Accuracy &#8211; is the ability to obtain samples which represent the true nature of the material supply.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Precision &#8211; is a statistical term relating to the number of samples taken from a lot or consignment.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Biomass is a highly variable product and requires a large number of samples in order to establish sampling precision.\u00a0 Precision can only be increased by increasing the number of spot samples.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">A single spot sample generally is less likely to be representative of the main body of biomass than is a gross sample, which is a mixture of multiple spot samples.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><strong>2.\u00a0 Sampling Bias<\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Poor sampling can induce systematic errors that skew the results. Two common errors are:<\/span><\/p>\n<ol type=\"a\">\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Spot samples are taken where certain properties are over-represented. eg. \u2013 at tail-gate of a truck where fines have settled to the bottom.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">The sample device is not capable of taking a representative sample. eg. \u2013 the sample device is too small and either rejects large pieces or overflows.<\/span><\/li>\n<\/ol>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Properly designed, operated and maintained automatic samplers can minimize systematic sampling bias.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Fractionation<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Fractionation or particle separation can occur from the way in which biomass is loaded \/ stacked and the way in which it is transported. eg. \u2013 fines will settle down to the bottom of a biomass truck over a long haul.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Additionally, fractionation can be produced by the sampling device itself; either by rejecting oversize pieces, failing to pick-up small particles, selectively picking up small particles, or breaking up particles by the sampling motion itself.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Stationary material is not uniform due to fractionation where material stratifies according to size. In order to get a representative gross sample from stationary material, a very large number of increment or spot samples are required.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><strong><span style=\"font-family: Arial;\">3.\u00a0 Classification of Sampling Techniques<\/span><\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">The quality of the sample depends upon the amount of human discretion involved, the sampling conditions, and the sampling location and timing.<\/span><\/p>\n<ol type=\"a\">\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Generally, those samples which do not involve human discretion are more accurate.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Accepted sampling conditions, include:<\/span><\/li>\n<\/ol>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Stopped Belt Cut (Laboratory Reference Method) &#8211; taking a full cross-section cut of material from off of a stopped conveyor belt.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Full Stream Cut \u2013 taking a full cross-section cut of material from a falling stream.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Partial Stream Cut \u2013 only taking a part of the cross-section of falling stream.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Stationary Sampling \u2013 taking a sample from a stationary pile or container.<\/span><\/li>\n<\/ul>\n<blockquote><p><span style=\"font-family: Arial; font-size: 12pt;\">Generally, the stopped belt cut provides the best sample but is impractical to use in a production setting.\u00a0 Full-stream cut and partial-stream cut samples can produce results which are representative of the main body of material, depending upon the sampling equipment design.\u00a0 Stationary sampling produces the poorest sample.<\/span><\/p><\/blockquote>\n<ol start=\"3\" type=\"a\">\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Sample location and timing<\/span><\/li>\n<\/ol>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Systematic \u2013 samples are taken evenly spaced in time or location.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Random \u2013 samples are taken randomly spaced in time or location.<\/span><\/li>\n<\/ul>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Systematic spacing generally provides better results. The challenge is to design a sampling system and procedure, which repetitively produces the most representative sample and is easy and practical to use.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><strong><span style=\"font-family: Arial;\">4.\u00a0 Establishing Sampling Procedures and Selecting Sampling Equipment<\/span><\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><img loading=\"lazy\" decoding=\"async\" class=\"alignleft\" src=\"\/wp-content\/uploads\/2010\/02\/cold_belt4.jpg\" alt=\"\" width=\"236\" height=\"217\" align=\"left\" border=\"1\" \/>Establishing sampling procedures and selecting sampling devices requires an understanding of the following:<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><em>Material Being Sampled<\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Biomass is highly variable in size, configuration and moisture content. It is relatively fragile and size is often an important factor, so care must be taken not to break the particles unnecessarily during sampling.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><em>Number and Size of Samples<\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">This depends upon the variability of the biomass and is usually determined by the plant technical department based on historical statistical results.\u00a0 Where new sources are coming on line, it can be expected that the number of samples required will be greater than for established sources, where historical data is available.\u00a0 Normal sample size required in the lab is 8-10 litres (~0.35 ft\u0456).<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><em>Sample Collection Method<\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">The best practical method should be used. The `stopped-belt, full-cut\u2019 method is the best, but is not practical.\u00a0 The `falling stream, full-cut\u2019 or `partial cut\u2019 are the next best methods.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><em><span style=\"font-family: Arial;\">Sample Distribution Through Lot<\/span><\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Sample increments must be distributed through the whole volume of the lot, so that any one particle has an equal chance of being selected.\u00a0 This is particularly important where `fractionation\u2019 has occurred due to fines segregation to one part of the lot \/ consignment.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><em>Characteristics and Movement of Sampling Device<\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">The opening of the sampling device must be large enough so as not to reject the largest possible piece and the capacity must be large enough to completely contain the sample without spillage.\u00a0 There should be no rejection by size of material or movement of the device through the material.\u00a0 There should be no contamination of the sample by the device.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Preferably, the sample device will pass through the entire cross-section of the stream so that each particle has an equal chance of being selected; or at least through a partial section that will contain all particle sizes within the stream.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Device speed through the flow is critical as the device must not block the flow of material. The sampling device shall be non-clogging, self-cleaning and shall be designed to facilitate inspection and maintenance.\u00a0 Ideally, it will not be complex or costly to purchase and maintain.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><em>Location of Sampling Equipment<\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Equipment shall be located where:<\/span><\/p>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">It can effectively take a representative sample.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">It is convenient and readily accessible for sample taking.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">It is readily accessible for maintenance and inspection.<\/span><\/li>\n<\/ul>\n<p><span style=\"font-family: Arial; font-size: 12pt;\"><em>Maintenance of Sampling Equipment<\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Sampling equipment must be safely and readily accessible to enable inspection, cleaning and maintenance.\u00a0 Worn mechanical sampling equipment can produce biased results, therefore it is imperative that equipment is inspected, repaired when necessary, and the performance measured regularly.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><em><span style=\"font-family: Arial;\">Preservation of Moisture Content<\/span><\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">The sampling device \/ method shall neither dry the biomass out or add moisture.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><em><span style=\"font-family: Arial;\">Personnel<\/span><\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Sampling personnel shall be properly trained and qualified.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><em><span style=\"font-family: Arial;\">Criteria of Sampling Performance<\/span><\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Sampling procedures and equipment must be routinely monitored to ensure that the samples being collected are:<\/span><\/p>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Unbiased<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Accurate<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Provide the degree of precision required<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Representative of the whole lot<\/span><\/li>\n<\/ul>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">In addition, a constant sampling ratio should be maintained; ie. \u2013 constant volume or weight of sample as compared to the whole lot.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><em><span style=\"font-family: Arial;\">Sample Handling<\/span><\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Samples once collected must be:<\/span><\/p>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Clearly labeled and identified<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Sealed in moisture-proof containers<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Stored in a cool, dry place<\/span><\/li>\n<\/ul>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Samples properly stored in this manner can be kept in storage for up to 36 hours with no appreciable moisture loss.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><em><span style=\"font-family: Arial;\">Gross Sample Size Reduction<\/span><\/em><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Normal increment sample size as collected will be 8-10 litres (average bucket size); therefore, combined multiple increments (the gross sample) must be reduced down to the laboratory sample size in a manner that retains biomass representative of the whole lot.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Large gross samples shall be thoroughly mixed before being reduced to laboratory sample size.<br \/>\nLarge samples can be reduced in size by mixing thoroughly and coning and quartering or by the use of an automatic splitter.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><strong><span style=\"font-family: Arial;\"><img loading=\"lazy\" decoding=\"async\" class=\"alignleft\" src=\"\/wp-content\/uploads\/2010\/02\/janze_sampling2.jpg\" alt=\"\" width=\"159\" height=\"240\" align=\"left\" border=\"1\" \/>5. Design of Sampling Equipment<\/span><\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">There are many `off-the-shelf\u2019 product samplers; most of which were designed for materials other than biomass. However, it is the author\u2019s experience that the best sampling equipment is custom designed to meet the specific requirements of the biomass sampling application considering the sampling requirements described in this paper, the product being handled, and the physical and operational constraints.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">(Photo:\u00a0 Wood Chip Sampler)<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><strong><span style=\"font-family: Arial;\">Summary<\/span><\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">To be of value, biomass samples need to be unbiased, accurate, precise and representative of the main lot or consignment of biomass.\u00a0 Biomass is highly variable in size, configuration and moisture content and is prone to fractionation and stratification, which complicate the sampling procedure.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Single spot \/ increment samples tend not to be accurate or representative of the main lot \/ consignment, particularly those samples taken from stationary loads or piles where fractionation has occurred.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Two common sampling errors, which bias results are:<\/span><\/p>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Spot samples are taken where certain properties are over-represented. eg. \u2013 at the tail-gate of a truck where fines have settled to the bottom.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">The sample device is not capable of taking a representative sample. ie. \u2013 the sample device is too small and either rejects large pieces or overflows.<\/span><\/li>\n<\/ul>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">The best, practical sampling procedures and equipment have the following features:<\/span><\/p>\n<ul>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Human discretion is minimized.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Full-stream cut or partial-stream cut sampling is employed.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Samples are taken systematically in time and \/or location throughout the whole volume of the main lot \/ consignment.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">They do not introduce bias or contaminants into the sample.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">They are convenient to use.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Preferably, they automatically reduce the gross sample to the laboratory sample size.<\/span><\/li>\n<li><span style=\"font-family: Arial; font-size: 12pt;\">Preferably, they have low capital and maintenance costs.<\/span><\/li>\n<\/ul>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">It is not easy to achieve all of these objectives, however, the primary goals of accuracy, precision and representativeness must take precedence.\u00a0 Convenience and cost, while important, are secondary considerations.<\/span><\/p>\n<p><span style=\"font-size: 12pt;\"><strong><span style=\"font-family: Arial;\">About our author<\/span><\/strong><\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Paul Janze is a senior material handling specialist with more than 30 years experience in engineering, equipment design and manufacture, project management and plant maintenance, primarily in the forest products industry. He is a specialist with difficult-to-handle materials such as wood chips, hog fuel, wastewood and bark, biosolids sludge and wet pulp, poultry litter and boiler ash which all have differing and unique handling characteristics.<\/span><\/p>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">For more information contact:<\/span><\/p>\n<blockquote><p><span style=\"font-family: Arial; font-size: 12pt;\">Mr. Paul Janze<br \/>\nMaterial Handling Specialist<br \/>\nSandwell Engineering Inc.<br \/>\n885 Dunsmuir Street, Suite 600<br \/>\nVancouver, BC,\u00a0 V6C-1N5<br \/>\nCanada<br \/>\nTelephone: 604-684-9311<br \/>\nFax: 604-688-5913<br \/>\nEmail:\u00a0<a href=\"mailto:pjanze@sandwell.com\">pjanze@sandwell.com<\/a><br \/>\nWeb site:\u00a0<a href=\"http:\/\/www.sandwell.com\/\">http:\/\/www.sandwell.com\/<\/a><\/span><\/p><\/blockquote>\n<p><span style=\"font-family: Arial; font-size: 12pt;\">Guest articles for the Ask Joe! Column are always welcome, for more information please contact Joe Marinelli directly at his email address:\u00a0\u00a0<a href=\"mailto:joe@solidshandlingtech.com\">joe@solidshandlingtech.com<\/a>.<\/span><\/p>\n<p>&nbsp;<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Requirements for Biomass Sampling Guest article by Paul Janze, Sandwell Engineering Introduction With the current emphasis on the use of biomass for `green\u2019 energy purposes, the importance of having good quality `hog fuel\u2019, cannot be over-emphasized. And to ensure good quality fuel, good sampling procedures must be followed. Woody biomass in chip form has been [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_monsterinsights_skip_tracking":false,"footnotes":""},"categories":[2],"tags":[15],"class_list":["post-117","post","type-post","status-publish","format-standard","hentry","category-articles","tag-sampling"],"_links":{"self":[{"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=\/wp\/v2\/posts\/117","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=117"}],"version-history":[{"count":3,"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=\/wp\/v2\/posts\/117\/revisions"}],"predecessor-version":[{"id":444,"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=\/wp\/v2\/posts\/117\/revisions\/444"}],"wp:attachment":[{"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=117"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=117"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/solidshandlingtech.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=117"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}